SINTESIS DAN KARAKTERISASI SILIKA GEL DARI LIMBAH KACA SERTA APLIKASINYA PADA KROMATOGRAFI KOLOM

Authors

  • Verry Andre Fabiani Jurusan Kimia, Fakultas Teknik, Universitas Bangka Belitung
  • Nelly Wahyuni Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Tanjungpura
  • Ridho Brilliantoro Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Tanjungpura
  • Mellisa Nurul Safitri Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Tanjungpura

DOI:

https://doi.org/10.26418/indonesian.v1i1.26038

Abstract

Silica gel synthesis from glass waste have been carried out with activation and purification method by using hydrochloride acid. Hydrochloride acid were varied 8 N, 10 N, and 12 N to observe optimum concentration in purification of silica gel and component separation in chromatography column. Gravimetric analysis result showed 12 N hydrochloride acid produce ~100 % silica. XRD and FTIR analysis revealed that synthetic gel silica was amorphous where its IR absorption bands were at 3426 cm-1, 1620 cm-1, 1080 cm-1, 772 cm-1 and 478 cm-1. The absorption bands agreed to standard gel silica and spectrum. The most effective HCl in gel silica synthesis was 12 N, caused by its ability to separate color component in a column. The synthetic silica that can be applied as stationary phase in column chromatography.

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Published

2018-07-23

Issue

Vol. 1 No. 1 (2018)

Section

Articles

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Copyright (c) 2018 Verry Andre Fabiani, Nelly Wahyuni, Ridho Brilliantoro, Mellisa Nurul Safitri

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