SINTESIS DAN STUDI STABILITAS NANOPARTIKEL PERAK TERTUDUNG ASAM SALISILAT

Authors

  • Rizky Noviani Ridwan Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Tanjungpura
  • Gusrizal Gusrizal Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Tanjungpura
  • Nurlina Nurlina Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Tanjungpura
  • Sri Juari Santosa Departemen Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Gadjah Mada

DOI:

https://doi.org/10.26418/indonesian.v1i3.34195

Abstract

Silver nanoparticles capped with salicylic acid have been synthesized by reduction of silver nitrate with salicylic acid without additional capping agent. In the formation of silver nanoparticles, the solution of silver nitrate was first mixed with the pH 11 salicylic acid solutions at a mole ratio of 1:40. The mixture was heated for 45 minutes in a boiling water bath. The formation of silver nanoparticles was indicated by the appearance of yellow color and monitored using UV-Vis spectrophotometer. The maximum peak of resulted silver nanoparticles appeared in the range of 410-420 nm with the average size of particles was 66 ±28 nm. Stability test over a period of 16 weeks showed that silver nanoparticles capped with salicylic acid were stable. The results of stability test show that salicylic acid simultaneously act as reducing as well as capping agent in the formation of silver nanoparticles.

References

Singh, D., Rathod, V., Ninganagouda, S., Hiremath, J., Singh, A.K., Mathew, J., Optimization and Characterization of Silver Nanoparticle by Endophytic Fungi Penicillium sp. Isolated from Curcuma longa (Turmeric) and Application Studies Against MDR E. coli and

S. aureus. Bioinorganic Chemistry and Applications. 2014; 2014: 1-8.

Sulistiawaty, L., Sugiarti, S., Darmawan, N., Detection of Hg+2 Metal Ions Using Silver Nanoparticles Stabilized by Gelatin and Tween-20. Indonesian Journal of Chemistry. 2015; 15(1): 1-8.

Wahyudi, T., Sugiana, D., Helmy, Q., Sintesis Nanopartikel Perak dan Uji Aktivitasnya terhadap Bakteri E. coli dan S. aureus. Arena Tekstil. 2011; 26(1): 1-60.

Saputra, A.H., Haryono, A., Laksmono, J.A., Anshari, M.H., Preparasi Koloid Nanosilver dengan Berbagai Jenis Reduktor sebagai Bahan Anti Bakteri. Jurnal Sains Materi Indonesia. 2011; 12(3): 202-208.

Junaidi, A.B., Wahyudi, A., Umaningrum, D., Sintesis AgNPs Secara Reduksi Kimia Menggunakan Capping Agent Kitosan dan Pereduksi Glukosa. Sains dan Terapan Kimia. 2015; 9(2): 70-80.

Apriandanu, D.O.B., Wahyuni, S., Hadisaputro, S., Harjono., Sintesis Nanopartikel Perak Menggunakan Metode Poliol dengan Agen Stabilisator Polivinilalkohol (PVA). Jurnal MIPA. 2013; 36 (2): 157-168.

Annadhasan, M., Muthukumarasamyvel, T., Babu Sankar, V.R., Rajendiran, N., Green Synthesized Silver and Gold Nanoparticles for Colorimetric Detection of Hg2+, Pb2+ and Mn2+ in Aqueous Medium. ACS Sustainable Chemistry Engineering. 2014; 2(4): 887-896.

Gusrizal, G., Santosa, S.J., Kunarti, E.S., Rusdiarso, B., Dual Function of p-Hydroxybenzoic Acid as Reducing and Capping Agent in Rapid and Simple Formation of Stable Silver Nanoparticles. International Journal of ChemTech Research. 2016; 9(8): 472- 482.

Gusrizal, G., Santosa, S.J., Kunarti, E.S., Rusdiarso, B., Synthesis of Silver Nanoparticles by Reduction of Silver Ion with m-Hydroxybenzoic Acid. Asian Journal of Chemistry. 2017; 29(7): 1417-1422.

Gusrizal, G., Santosa, S.J., Kunarti, E.S., Rusdiarso, B., Two Highly Stable Silver Nanoparticles: Surface Plasmon Resonance Spectra Study of Silver Nanoparticles Capped with m-Hydroxybenzoic Acid and p-Hydroxybenzoic Acid. Molekul. 2018; 13(1): 30-37.

Baghizadeh, A., Ranjbar, S., Gupta, V.K., Asif, M., Pourseyedi, S., Karimi, M.J., Mohammadinejad R., Green Synthesis of Silver Nanoparticles Using Seed Extract of Calendula officinalis in Liquid Phase. Journal of Molecular Liquids. 2015; 207: 159-163.

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Published

2019-07-12

Issue

Vol. 1 No. 3 (2018)

Section

Articles

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Copyright (c) 2019 Rizky Noviani Ridwan, Gusrizal Gusrizal, Nurlina Nurlina, Sri Juari Santosa

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